Determination of Total Specific Migration of Acrylic Acid and Acrylic Esters in Food Contact Materials

Meng Qing, Honzhen Zhang, Qingyun Xia, Bohen Huang

Abstract

In this study, we selected a total specific migration indicator including 12 acrylic acid and acrylic esters, i.e. SML (T) 22 from national food safety standard. After comparison, methyl acetate was selected as the extracting agent, which was applicable for the treatment of acidic and aqueous simulants. The HP - INNOWAX polarity column was applied to separate the 12 compounds and the solvent. The GC - MS was utilized for qualitative and quantitative analysis with optimization of extraction duration, temperature program, scanning mode as well as the carrier gas flow rate and the sampling volume. The 12 acrylic compounds present good separation in 12 minutes, and the analytical duration is greatly shortened. The linearities in different simulants range from 0.047 mg/L to 11.43 mg/L, while the detection limits are from 0.009 mg/L to 0.666 mg/L. The actual products analysis shows that the recoveries are between 81.2% and 81.2%, and the RSDs (n = 6) are within 5.15%. This developed analysis method is fast, economical, non-toxic, with low detection limit, high precision and high accuracy. It has good applicability and is easy to promote to use.

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Paper Citation


in Harvard Style

Qing M., Zhang H., Xia Q. and Huang B. (2018). Determination of Total Specific Migration of Acrylic Acid and Acrylic Esters in Food Contact Materials.In Proceedings of the 2nd International Conference on Intelligent Manufacturing and Materials - Volume 1: ICIMM, ISBN 978-989-758-345-2, pages 529-536. DOI: 10.5220/0007535105290536


in Bibtex Style

@conference{icimm18,
author={Meng Qing and Honzhen Zhang and Qingyun Xia and Bohen Huang},
title={Determination of Total Specific Migration of Acrylic Acid and Acrylic Esters in Food Contact Materials},
booktitle={Proceedings of the 2nd International Conference on Intelligent Manufacturing and Materials - Volume 1: ICIMM,},
year={2018},
pages={529-536},
publisher={SciTePress},
organization={INSTICC},
doi={10.5220/0007535105290536},
isbn={978-989-758-345-2},
}


in EndNote Style

TY - CONF

JO - Proceedings of the 2nd International Conference on Intelligent Manufacturing and Materials - Volume 1: ICIMM,
TI - Determination of Total Specific Migration of Acrylic Acid and Acrylic Esters in Food Contact Materials
SN - 978-989-758-345-2
AU - Qing M.
AU - Zhang H.
AU - Xia Q.
AU - Huang B.
PY - 2018
SP - 529
EP - 536
DO - 10.5220/0007535105290536