Synthesis of 1-Nitronaphthalene under Homogeneous Conditions

Yuriy G. Khabarov, Viacheslav A. Veshnyakov, Ivan A. Snigirev, Ilya I. Pikovskoy

Abstract

Various reagents can be used for the nitration of naphthalene ranging from the classical nitrating mixture to unusual reagent systems. In this study, a simple and effective method of nitration of naphthalene using a classical nitrating mixture in 1,4-dioxane is presented. The reaction occurs under homogeneous conditions and GC-MS analysis of the product showed 2 peaks corresponding to 1-nitronaphthalene (96%) and 2-nitronaphthalene (4%). Melting point, UV and IR spectra of the product (isolated in 96-97% yields) correspond to 1-nitronaphthalene.

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Paper Citation


in Harvard Style

Khabarov Y., Veshnyakov V., Snigirev I. and Pikovskoy I. (2018). Synthesis of 1-Nitronaphthalene under Homogeneous Conditions.In The Second International Conference on Materials Chemistry and Environmental Protection - MEEP, ISBN 978-989-758-360-5, pages 73-76. DOI: 10.5220/0008185800730076


in Bibtex Style

@conference{meep18,
author={Yuriy G. Khabarov and Viacheslav A. Veshnyakov and Ivan A. Snigirev and Ilya I. Pikovskoy},
title={Synthesis of 1-Nitronaphthalene under Homogeneous Conditions},
booktitle={The Second International Conference on Materials Chemistry and Environmental Protection - MEEP,},
year={2018},
pages={73-76},
publisher={SciTePress},
organization={INSTICC},
doi={10.5220/0008185800730076},
isbn={978-989-758-360-5},
}


in EndNote Style

TY - CONF

JO - The Second International Conference on Materials Chemistry and Environmental Protection - MEEP,
TI - Synthesis of 1-Nitronaphthalene under Homogeneous Conditions
SN - 978-989-758-360-5
AU - Khabarov Y.
AU - Veshnyakov V.
AU - Snigirev I.
AU - Pikovskoy I.
PY - 2018
SP - 73
EP - 76
DO - 10.5220/0008185800730076